Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Aminobenzoic Acid → HCID 67078597, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Aminobenzoic Acid | HCID 978 | — |
| 반응물 | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| 반응물 | 3,4,5-Trimethoxybenzylamine | HCID 87736 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | HCID 67078597 | HCID 67078597 | 94.6% |
반응 단계
N,N-carbonyldiimidazole (1.62 g, 10 mmol), 3,4,5-trimethoxybenzyl amine (1.97 g, 10 mmol), p-aminobenzoic acid (1.52 g, 10 mmol), and 10 ml of 1 mol/L sodium hydroxide are used according to the method for the production of compound III in Method two to obtain 3.54 g of 4-[(3,4,5-trimethoxybenzylureido)methyl]benzoic acid (intermediate M-35) as a white solid, with a yield of 94.6%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08889876B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-3d01f9b77e7e44969a51c2bde6985c6f |
| 출처 메모 | uspto-grants-2014_11 |