Hydrochloric Acid → HCID 178418457, 화합물
반응식
[C:1]([C:4]1[CH:5]=[C:6]([CH:8]=[C:9]([C:11](=[O:13])[CH3:12])[CH:10]=1)[NH2:7])(=[O:3])[CH3:2].[C:14]([NH:16][C:17]([NH2:19])=[NH:18])#[N:15].[ClH:20]>O>[ClH:20].[C:1]([C:4]1[CH:5]=[C:6]([NH:7][C:14]([NH:16][C:17]([NH2:19])=[NH:18])=[NH:15])[CH:8]=[C:9]([C:11](=[O:13])[CH3:12])[CH:10]=1)(=[O:3])[CH3:2]참가 물질
5
실험 절차
Compound No. 12. A suspension of 3,5-diacetylaniline (0.531 g) in water (8 mL) was treated with cyanoguanidine (0.285 g) and conc. HCl (0.25 mL) and heated at reflux. After 6 hr the mixture was cooled and concentrated and 0.248 g of off-white solid was filtered out and dried to give N-(3,5-diacetylphenyl)biguanide hydrochloride, mp 260°-70° C. (dec).
후처리
- temperatureheated
- temperatureat reflux
- temperatureAfter 6 hr the mixture was cooled
- concentrationconcentrated
- filtration0.248 g of off-white solid was filtered out
- customdried
출처 및 근거
- ORD 기록
- ord-705eb0cf3a5441248217ccc079f91152
- 출처 데이터셋
- uspto-grants-1998_03
- 특허 번호
- US05733932
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