Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Aminotetralin, (R)- → HCID 86705881, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Aminotetralin, (R)- | HCID 7058072 | — |
| 반응물 | N-Carbobenzyloxy-4-keto-L-proline | HCID 11076282 | — |
| 반응물 | HCID 86705863 | HCID 86705863 | — |
| 생성물 | HCID 86705881 | HCID 86705881 | 100% |
반응 단계
Following a procedure analogous to that for the synthesis of Compound D of Example 1, (S)-1-((benzyloxy)carbonyl)-4-oxopyrrolidine-2-carboxylic acid (Aldrich, 4.00 g, 15.2 mmol) and (R)-1,2,3,4-tetrahydronaphthalen-1-amine (Alfa Aesar, 2.23 mL, 15.2 mmol) were converted to the title compound (5.96 g, 100%). MS (ESI+) m/z 393.1 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08889712B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-b57b0c004422490bb033116c448e77a6 |
| 출처 메모 | uspto-grants-2014_11 |