Sodium Hydroxide → Sodium 6-methoxynicotinate

HRID 339380

반응식

HRID 339380 반응식
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([O:9]C)=[O:8])=[CH:5][N:4]=1.[OH-].[Na+:14]>O1CCOCC1>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([O-:9])=[O:8])=[CH:5][N:4]=1.[Na+:14]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 586039Methyl 6-methoxypyridine-3-carboxylate

생성물 1

HCID 23717611Sodium 6-methoxynicotinate

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

methyl 6-methoxynicotinate (2.097 g, 12.56 mmol) was dissolved in dioxane (30 mL). An aqueous solution of NaOH (1.0N, 25 mL) was added to the solution and the mixture was stirred at room temperature overnight. The solvent was removed under reduced pressure to provide 2.2 g of sodium 6-methoxynicotinate.

후처리

  1. customThe solvent was removed under reduced pressure

출처 및 근거

ORD 기록
ord-0482b300a3214a2a9e2d4a88299a8574
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08895050B2

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