Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → HCID 178447967, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | HCID 178447942 | HCID 178447942 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | HCID 178418361 | HCID 178418361 | — |
| 생성물 | HCID 178447967 | HCID 178447967 | 63.2% |
반응 단계
To a liquid mixture comprising 250 ml of ethanol and 250 ml of toluene was dissolved 92 g of the (4-(2-(trans-4-n-propylcyclohexyl)ethyl)cyclohexene-1-yl)benzene mentioned above, 5 g of palladium/carbon (5%) was added as catalyst thereto, and they were subjected to a catalytic reduction in hydrogen gas atmosphere. After finishing of the reaction, the catalyst was filtered off and the solvent was distilled off under a reduced pressure to obtain a yellow oily product. This product was recrystallized from ethanol to obtain 58.5 g of (trans-4-(2-(trans-4-n-propylcyclohexyl)ethyl)cyclohexyl)benzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05858275 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-e2e2f4eab272414ebdf8b504cd6d8980 |
| 출처 메모 | uspto-grants-1999_01 |