Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Azobisisobutyronitrile → 4-(Chloromethyl)benzophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | 4-Methylbenzophenone | HCID 8652 | — |
| 반응물 | Chlorine | HCID 24526 | — |
| 용매 | Chlorobenzene | HCID 7964 | — |
| 생성물 | 4-(Chloromethyl)benzophenone | HCID 3016376 | — |
반응 단계
196.2 g of 4-methylbenzophenone are dissolved in chlorobenzene and then gassed at 80° C. in the presence of 1.6 g of AIBN (azodiisobutyronitrile) with a total of 71.0 g of chlorine. The reaction mixture is concentrated and the solid material obtained recrystallized from 1 L of ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05859084 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-e7340966d1a240309ff577fc36a68f15 |
| 출처 메모 | uspto-grants-1999_01 |