反应详情

196.2 g of 4-methylbenzophenone are dissolved in chlorobenzene and then gassed at 80° C. in the presence of 1.6 g of AIBN (azodiisobutyronitrile) with a total of 71.0 g of chlorine. The reaction mixture is concentrated and the solid material obtained recrystallized from 1 L of ethanol.

1. concentrationThe reaction mixture is concentrated
2. customthe solid material obtained
3. customrecrystallized from 1 L of ethanol