4-(N-formylaminomethyl)benzophenone → (4-(Aminomethyl)phenyl)(phenyl)methanone

HRID 342792

반응식

HRID 342792 반응식
C([NH:3][CH2:4][C:5]1[CH:18]=[CH:17][C:8]([C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:10])=[CH:7][CH:6]=1)=O>Cl.C(O)C>[NH2:3][CH2:4][C:5]1[CH:18]=[CH:17][C:8]([C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:10])=[CH:7][CH:6]=1

참가 물질

4

반응물 1

HCID 537210824-(N-formylaminomethyl)benzophenone

생성물 1

HCID 2760963(4-(Aminomethyl)phenyl)(phenyl)methanone

시약·촉매·용매 2

HCID 313Hydrochloric Acid용매HCID 702Ethanol용매

실험 절차

70 g of 4-(N-formylaminomethyl)benzophenone are stirred in a mixture of 40 g of concentrated hydrochloric acid and 100 g of ethanol for 5 hours at 50° C. The alcohol is then removed by distillation and the pH is adjusted to 10 with sodium hydroxide solution. 4-aminomethylbenzophenone precipitates as an oil.

후처리

  1. customThe alcohol is then removed by distillation
  2. custom4-aminomethylbenzophenone precipitates as an oil

출처 및 근거

ORD 기록
ord-8df23931cdc646c2a417537deeb17402
출처 데이터셋
uspto-grants-1999_01
특허 번호
US05859084

연결된 노트

불러오는 중…