Ethyl p-methylbenzenesulfonate → HCID 86745143, 화합물

HRID 345199노트

반응식

HRID 345199 반응식
[C:1]1([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:6]=[CH:5][C:4]([C:7]2[N:8]=[C:9]([CH3:12])[S:10][CH:11]=2)=[CH:3][CH:2]=1.[C:19]1([CH3:31])[CH:24]=[CH:23][C:22]([S:25]([O:28]CC)(=[O:27])=[O:26])=[CH:21][CH:20]=1>>[C:1]1([C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:6]=[CH:5][C:4]([C:7]2[N+:8]([CH2:19][CH3:20])=[C:9]([CH3:12])[S:10][CH:11]=2)=[CH:3][CH:2]=1.[CH3:31][C:19]1[CH:24]=[CH:23][C:22]([S:25]([OH:28])(=[O:27])=[O:26])=[CH:21][CH:20]=1

참가 물질

3

반응물 2

HCID 6638Ethyl p-methylbenzenesulfonateHCID 906354-(4-Biphenylyl)-2-methylthiazole

생성물 1

HCID 86745143HCID 86745143, 화합물

실험 절차

4-(Biphenyl-4-yl)-2-methyl-thiazole (9.8 pbw) and ethyl p-toluenesulfonate (8.6 pbw) are stirred for 3 hours at 180° C. The hot mixture is poured onto acetone and further processed as described in Preparation Example 5(a).

후처리

  1. additionThe hot mixture is poured onto acetone
  2. customas described in Preparation Example 5(a)

출처 및 근거

ORD 기록
ord-f59042f79eae4811a8b040d8b0813e3c
출처 데이터셋
uspto-grants-1991_10
특허 번호
US05055579

반응 노트

불러오는 중…