Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibenzylhydroxylamine → Carbamic acid, N-[3-[[[[[bis(phenylmethyl)amino]oxy]carbonyl]amino]methyl]-3,5,5-trimethylcyclohexyl]-, bis(phenylmethyl)azanyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibenzylhydroxylamine | HCID 69297 | — |
| 반응물 | Isophorone diisocyanate | HCID 169132 | — |
| 생성물 | Carbamic acid, N-[3-[[[[[bis(phenylmethyl)amino]oxy]carbonyl]amino]methyl]-3,5,5-trimethylcyclohexyl]-, bis(phenylmethyl)azanyl ester | HCID 15180716 | — |
반응 단계
The procedure of Example 1 is repeated using 10.66 g (50 mmol) of N,N-dibenzylhydroxylamine and 5.56 g (25 mmole) of 3-isocyanatomethyl-3,5,5-trimethylcyclohexylisocyanate. The residue is recrystallized from a 1:1 heptane: toluene solvent mixture to give 11.0 g (68%) of a white soldi, m.p. 139°-146° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05057610 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-095f55741929481cb0eafb9e9807fb1f |
| 출처 메모 | uspto-grants-1991_10 |