1,4-Dibromobutane → HCID 22314024, 화합물

반응식

[F:1][C:2]([F:20])([F:19])[C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:13]3[CH:14]=[CH:15][C:16]([OH:18])=[CH:17][C:12]=3[S:11][N:10]=2)=[CH:5][CH:4]=1.[Br:21][CH2:22][CH2:23][CH2:24][CH2:25]Br>>[Br:21][CH2:22][CH2:23][CH2:24][CH2:25][O:18][C:16]1[CH:15]=[CH:14][C:13]2[C:9]([C:6]3[CH:5]=[CH:4][C:3]([C:2]([F:1])([F:19])[F:20])=[CH:8][CH:7]=3)=[N:10][S:11][C:12]=2[CH:17]=1

참가 물질

반응물 2

HCID 80561,4-Dibromobutane

HCID 135847955HCID 135847955, 화합물

생성물 1

HCID 22314024HCID 22314024, 화합물

실험 절차

In analogy to example 2.1, 3-(4-Trifluoromethyl-phenyl)-benzo[d]isothiazol-6-ol and 1,4-dibromobutane were converted to yield 6-(4-Bromo-butoxy)-3-(4-trifluoromethyl-phenyl)-benzo[d]isothiazole as light yellow solid, MS: 429 (M, 1Br).

출처 및 근거

ORD 기록: ord-33e0b5da711946fd8f300d17e7f50fdf
출처 데이터셋: uspto-grants-2007_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07173043B2

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