Sulfuric Acid → HCID 178512812, 화합물

HRID 34751

반응식

HRID 34751 반응식
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].CS[C:11](=[NH:13])[NH2:12].OS(O)(=O)=O>O>[NH:1]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][NH2:8])[C:11]([NH2:13])=[NH:12]

참가 물질

5

반응물 3

HCID 1118Sulfuric AcidHCID 51422-Methyl-2-thiopseudoureaHCID 16402Hexamethylenediamine

생성물 1

HCID 178512812HCID 178512812, 화합물

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

To 2.3 g. of 1,6-diaminohexane dissolved in 50 ml. of H2O was added dropwise with vigorous stirring a solution of 2 g. of S-methylthiopseudourea.H2SO4 in 20 ml. of H2O. After the completion of addition, the stirring was continued for 15 hours, after which the precipitate (the diadduct) was filtered. The filtrate was concentrated to a viscous oil which upon the addition of 50 ml. of MeOH precipitated 718 mg. of white powder.

후처리

  1. additionAfter the completion of addition
  2. filtrationafter which the precipitate (the diadduct) was filtered
  3. concentrationThe filtrate was concentrated to a viscous oil which upon the addition of 50 ml
  4. customof MeOH precipitated 718 mg

출처 및 근거

ORD 기록
ord-9cf58c54b4b744f8a9806c38daf1df95
출처 데이터셋
uspto-grants-1988_08
특허 번호
US04762949

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