Potassium Carbonate → 4-((Allyl(methyl)amino)methyl)thiazol-2-amine
반응식
[CH2:1]([NH:4][CH3:5])[CH:2]=[CH2:3].Cl.[NH2:7][C:8]1[S:9][CH:10]=[C:11]([CH2:13]Cl)[N:12]=1.C(=O)([O-])[O-].[K+].[K+]>C(O)C>[CH2:1]([N:4]([CH2:13][C:11]1[N:12]=[C:8]([NH2:7])[S:9][CH:10]=1)[CH3:5])[CH:2]=[CH2:3]참가 물질
5
실험 절차
N-allyl-N-methylamine (7.0 mg, 0.1 mmol), 2-amino-4-chloromethylthiazole hydrochloride (18.5 mg, 0.1 mmol), and potassium carbonate (30 mg, 0.21 mmol) are shaken in ethanol (1 mL) at room temperature for 18 hours. The mixture is filtered and the filtrate was condensed under vacuum.
후처리
- filtrationThe mixture is filtered
- customcondensed under vacuum
출처 및 근거
- ORD 기록
- ord-6de76e9d87074e8c81db3041feaa73dd
- 출처 데이터셋
- uspto-grants-2007_02
- 특허 번호
- US07183300B2
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