Acrylonitrile → 1-Pyrrolidinepropionitrile

HRID 351489노트

반응식

HRID 351489 반응식
[C:1](#[N:4])[CH:2]=[CH2:3].[NH:5]1[CH2:9][CH2:8][CH2:7][CH2:6]1>>[N:5]1([CH2:3][CH2:2][C:1]#[N:4])[CH2:9][CH2:8][CH2:7][CH2:6]1

참가 물질

3

반응물 2

HCID 7855AcrylonitrileHCID 31268Pyrrolidine

생성물 1

HCID 1177431-Pyrrolidinepropionitrile

실험 절차

At 20 to 30° C., 5.31 g of acrylonitrile was added to 7.11 g of pyrrolidine, which was stirred for 2 hours. Purification by vacuum distillation yielded 1-pyrrolidine-propiononitrile.

후처리

  1. customPurification
  2. distillationby vacuum distillation

출처 및 근거

ORD 기록
ord-8eb4190cc02c421da9ccea55598b59b1
출처 데이터셋
uspto-grants-2004_06
특허 번호
US06743564B2

반응 노트

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