Sodium Hydroxide → Sodium orthosilicate

반응식

[O-:1][Si:2]([O-:4])=[O:3].[Na+:5].[Na+].[OH-:7].[Na+]>>[Si:2]([O-:7])([O-:4])([O-:1])[O-:3].[Na+:5].[Na+:5].[Na+:5].[Na+:5]

참가 물질

반응물 2

HCID 14798Sodium Hydroxide

HCID 23266Sodium Silicate

생성물 1

HCID 26051Sodium orthosilicate

실험 절차

50 kg of water glass having an SiO2/Na2O ratio of 2.06 and an active substance content of 45.5% were admixed with 0.612 kg of sodium hydroxide solution (48% strength) and spray-dried in a laboratory spray dryer (spray tower) from Anhydro to give an amorphous sodium silicate with an active substance content of 84%. 15 kg of the amorphous sodium silicate are heat-treated at 720° C. for 90 min in a muffle furnace (Nabertherm, model W1000/H). The chilled material (about 10 kg) is pulverized using a jaw crusher and a disk mill.

후처리

customspray-dried in a laboratory spray dryer (spray tower) from Anhydro

출처 및 근거

ORD 기록: ord-74b702d16a8e480ebba09ab227727942
출처 데이터셋: uspto-grants-2004_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06743766B1

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