Sodium Hydroxide → HCID 15612245, 화합물

HRID 35196노트

반응식

HRID 35196 반응식
Cl.[N:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][C:9]2[CH:18]=[CH:17][C:16]3[C:11](=[CH:12][CH:13]=[C:14]([C:19]([OH:21])=[O:20])[CH:15]=3)[CH:10]=2)[CH:3]=1.[OH-].[Na+]>C(Cl)Cl>[N:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][C:9]2[CH:18]=[CH:17][C:16]3[C:11](=[CH:12][CH:13]=[C:14]([C:19]([OH:21])=[O:20])[CH:15]=3)[CH:10]=2)[CH:3]=1

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 704078322-(3-Pyridylmethyl)naphthalene-6-carboxylic acid hydrochloride

생성물 1

HCID 15612245HCID 15612245, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

A suspension of 2-(3-pyridylmethyl)naphthalene-6-carboxylic acid hydrochloride in 100 ml of methylene chloride is stirred with a stoichiometric amount of dilute aqueous sodium hydroxide solution until the salt is completely dissolved. The organic layer is separated, washed with water, dried over magnesium sulfate and evaporated to yield 2-(3-pyridylmethyl)naphthalene-6-carboxylic acid.

후처리

  1. dissolutionis completely dissolved
  2. customThe organic layer is separated
  3. washwashed with water
  4. dry with materialdried over magnesium sulfate
  5. customevaporated

출처 및 근거

ORD 기록
ord-3af67bb12ea247339371119e2a5e933d
출처 데이터셋
uspto-grants-1988_08
특허 번호
US04766127

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