HCID 20732811, 화합물 → HCID 14863951, 화합물
반응식
[CH3:1][O:2][CH:3]([O:19][CH3:20])[C@@H:4]1[CH2:8][CH2:7][CH2:6][N:5]1C(OCC1C=CC=CC=1)=O>CCO.[Ni]>[CH3:1][O:2][CH:3]([O:19][CH3:20])[CH:4]1[CH2:8][CH2:7][CH2:6][NH:5]1참가 물질
4
실험 절차
A solution of acetal 15 (5.8 9, 0.02 mol) in EtOH (50 mL) was allowed to stir for 16 hours at room temperature over Raney nickel (0.2 g), in order to remove the trace amounts of sulphur impurities prior to hydrogenation. Excess nickel was removed by filtration through Celite.
후처리
- customto remove the trace amounts of sulphur impurities
- customExcess nickel was removed by filtration through Celite
출처 및 근거
- ORD 기록
- ord-5ffbb9d8496a4c7691dc131f96ab5b1a
- 출처 데이터셋
- uspto-grants-2004_06
- 특허 번호
- US06747144B1
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