Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
DL-Carnitine → Cyclohexyl acetyl carnitine chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | DL-Carnitine | HCID 288 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Cyclohexylacetyl chloride | HCID 2757989 | — |
| 용매 | Trifluoroacetic acid | HCID 6422 | — |
| 생성물 | Cyclohexyl acetyl carnitine chloride | HCID 131715698 | — |
반응 단계
Carnitine chloride (2.97 g; 0.01 moles) was dissolved in trifluoro acetic acid (10 cc). To this solution was added cyclohexyl acetyl chloride (0.01 moles) prepared as previously disclosed and the resulting mixture was kept under stirring for 48 hours. Ethyl ether was then added and the resulting mixture was kept under stirring for 0.5 hours at 0° C. A precipitate was obtained, which was filtered off and dried under vacuum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04766222 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-ccb56ca24b4b4916a6432cb595293d2a |
| 출처 메모 | uspto-grants-1988_08 |