HRID35373

反应详情

EQUATION

反应方程式

HRID 35373 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Carnitine chloride (2.97 g; 0.01 moles) was dissolved in trifluoro acetic acid (10 cc). To this solution was added cyclohexyl acetyl chloride (0.01 moles) prepared as previously disclosed and the resulting mixture was kept under stirring for 48 hours. Ethyl ether was then added and the resulting mixture was kept under stirring for 0.5 hours at 0° C. A precipitate was obtained, which was filtered off and dried under vacuum.

WORKUP

后处理

  1. customprepared
  2. stirringunder stirring for 0.5 hours at 0° C
  3. customA precipitate was obtained
  4. filtrationwhich was filtered off
  5. customdried under vacuum