N,N'-Diethylthiourea → HCID 20506556, 화합물

HRID 354911

반응식

HRID 354911 반응식
[CH2:1]([NH:3][C:4]([NH:6][CH2:7][CH3:8])=[S:5])[CH3:2].[Br:9][CH2:10][C:11](=[O:25])[CH:12]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>CC(C)=O>[BrH:9].[C:13]1([CH:12]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:11]2([OH:25])[CH2:10][S:5][C:4](=[N:3][CH2:1][CH3:2])[N:6]2[CH2:7][CH3:8])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

참가 물질

4

반응물 2

HCID 2735009N,N'-DiethylthioureaHCID 27946353-Bromo-1,1-diphenylacetone

생성물 1

HCID 20506556HCID 20506556, 화합물

시약·촉매·용매 1

HCID 180Acetone용매2회

실험 절차

To a filtered solution of 1.32 g. of 1,3-diethyl-2-thiourea in 25 ml. of acetone is added a filtered solution of 3-bromo-1,1-diphenyl-2-propanone in 25 ml. of acetone. The mixture is allowed to stand, then the solid is collected by filtration, washed with acetone and dried in vacuo, giving 3.73 g. of the desired product, m.p. 174°-176° C. (dec.).

후처리

  1. filtrationthe solid is collected by filtration
  2. washwashed with acetone
  3. customdried in vacuo
  4. customgiving 3.73 g

출처 및 근거

ORD 기록
ord-2827049d555644459acdb2003933a016
출처 데이터셋
uspto-grants-1983_03
특허 번호
US04377589

연결된 노트

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