Hydrochloric Acid → HCID 15341898, 화합물

HRID 354914노트

반응식

HRID 354914 반응식
O1CCCCC1[O:7][C@H:8]1[CH2:13][CH2:12][C@H:11]2[C@H:14]3[C@H:24]([CH2:25][CH2:26][C@:9]12[CH3:10])[C@:22]1([CH3:23])[C@H:17]([C:18](=[O:27])[CH2:19][CH2:20][CH2:21]1)[CH2:16][CH2:15]3.Cl>C(O)C>[OH:7][C@H:8]1[CH2:13][CH2:12][C@H:11]2[C@H:14]3[C@H:24]([CH2:25][CH2:26][C@:9]12[CH3:10])[C@:22]1([CH3:23])[C@H:17]([C:18](=[O:27])[CH2:19][CH2:20][CH2:21]1)[CH2:16][CH2:15]3

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 1534189717beta-Tetrahydropyranyloxy-5alpha-androstan-4-one

생성물 1

HCID 15341898HCID 15341898, 화합물수율 116.7%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

To 75 ml of ethanol is added 2.32 g of the product of Step E to form a solution which is then treated with 5 ml of 2.5 N hydrochloric acid and warmed on a steam bath for 40 min. to yield 2.1 g of a crystalline product having a m.p. of 123°-126° C.

후처리

  1. customto form a solution which
  2. temperaturewarmed on a steam bath for 40 min.

출처 및 근거

ORD 기록
ord-7add9fb1d282489394e78ccb92ff4e39
출처 데이터셋
uspto-grants-1983_03
특허 번호
US04377584

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