Benzothiazolone → HCID 54205109, 화합물

HRID 355037

반응식

HRID 355037 반응식
[H-].[Na+].[S:3]1[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=2[NH:5][C:4]1=[O:12].[CH3:13][O:14][C:15](=[O:24])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]Br>CN(C=O)C>[CH3:13][O:14][C:15](=[O:24])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][N:5]1[C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[S:3][C:4]1=[O:12]

참가 물질

5

반응물 3

HCID 13625BenzothiazoloneHCID 24758Sodium hydrideHCID 11107373Methyl 8-bromooctanoate

생성물 1

HCID 54205109HCID 54205109, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

The product is produced as described in example 1 from 3 g. of NaH (80% suspension in mineral oil), 15.1 g. of benzthiazolin-2-one, 200 cc. of DMF, 23.7 g. of 8-bromo-caprylic acid methyl ester and 3 g. NaJ.

후처리

  1. customThe product is produced

출처 및 근거

ORD 기록
ord-addf4e48275b4874a28b8f3d64b11e27
출처 데이터셋
uspto-grants-1983_03
특허 번호
US04377695

연결된 노트

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