Hydrogen Bromide → 2-Benzyl benzylbromide

HRID 355768

반응식

HRID 355768 반응식
[CH2:1]([C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH2:10]O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[BrH:16]>>[CH2:1]([C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[CH2:10][Br:16])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 260Hydrogen BromideHCID 741092-Benzylbenzyl alcohol

생성물 1

HCID 124220982-Benzyl benzylbromide수율 98%

실험 절차

2-Benzylbenzyl alcohol (commercial) (1 g) was suspended in 48% aqueous hydrobromic acid (10 ml) and stirred vigorously for 20 hours. The resultant suspended solid was extracted twice with hexane and the extracts dried (MgSO4) and evaporated to give 2-benzyl benzylbromide as yellow solid (1.3 g, 98%).

후처리

  1. extractionwas extracted twice with hexane
  2. dry with materialthe extracts dried (MgSO4)
  3. customevaporated

출처 및 근거

ORD 기록
ord-93f2795254ed44abb88915047391a63e
출처 데이터셋
uspto-grants-1998_11
특허 번호
US05834468

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