Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3-Dimethylbenzoyl chloride → HCID 67623756, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3-Dimethylbenzoyl chloride | HCID 2800899 | — |
| 반응물 | 5-(4-Aminobenzoyl)-6,11-dihydro-5H-dibenz[b,e]azepine | HCID 15410467 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 67623756 | HCID 67623756 | 13.4% |
반응 단계
As described for Example 9, 0.628 g (2 mmol) of 5-(4-aminobenzoyl)-6,11-dihydro-5H-dibenz[b,e]azepine is reacted with 0.506 g (3.0 mmol) of 2,3-dimethylbenzoyl chloride in dichloromethane. The product is recrystallized from hexane-dichloromethane to give 0.12 g of crystals, m.p. 138°-142° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05834461 |
| 출처 데이터셋 | uspto-grants-1998_11 |
| ORD ID | ord-20d1bc6099d94f4b9ad4fa8e77c80f59 |
| 출처 메모 | uspto-grants-1998_11 |