Sodium cyanoborohydride → HCID 10750101, 화합물

HRID 356026노트

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HRID 356026 반응식
[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][C:10]=1[Cl:11])[NH:7][CH:6]=[CH:5]2.C([BH3-])#N.[Na+]>C(O)(=O)C>[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][C:10]=1[Cl:11])[NH:7][CH2:6][CH2:5]2

참가 물질

4

반응물 2

HCID 5003444Sodium cyanoborohydrideHCID 104877765,6-dichloro-1H-indole

생성물 1

HCID 10750101HCID 10750101, 화합물수율 90%

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

5,6-Dichloroindole (D38) was reduced in the usual way with sodium cyanoborohydride in glacial acetic acid to give the title compound (D39) (1.18 g, 90%).

출처 및 근거

ORD 기록
ord-fa896edfe4b34c0fa74014413e3506a2
출처 데이터셋
uspto-grants-1998_11
특허 번호
US05834494

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