Allylamine → 2,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]

HRID 359575

반응식

HRID 359575 반응식
[N:1]([C:10]([CH3:16])([CH3:15])[C:11]([O:13]C)=O)=[N:2][C:3]([CH3:9])([CH3:8])[C:4]([O:6]C)=O.[CH2:17]([NH2:20])[CH:18]=[CH2:19]>CO>[N:2]([C:3]([CH3:8])([CH3:9])[C:4]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:6])=[N:1][C:10]([CH3:16])([CH3:15])[C:11]([NH:20][CH2:17][CH:18]=[CH2:19])=[O:13]

참가 물질

4

반응물 2

HCID 7853AllylamineHCID 757631,1'-Dimethyl 2,2'-(1,2-diazenediyl)bis(2-methylpropanoate)

생성물 1

HCID 157247352,2'-Azobis[n-(2-propenyl)-2-methylpropionamide]

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Dimethyl 2,2'-azobis(2-methylpropionate) in an amount of 41.9 g, 48 ml of methanol, and 43 g of a 28% CH3ONa methanol solution were mixed and stirred for dissolution, followed by dropwise addition of 25 g of allylamine to react at 19° to 21° C. for 20 hours.

후처리

  1. customto react at 19° to 21° C. for 20 hours

출처 및 근거

ORD 기록
ord-cbc849f2079f4b2e89bfcd0e603da8a8
출처 데이터셋
uspto-grants-1991_03
특허 번호
US05001228

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