Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl benzoylacetate → N-(6-methoxybenzothiazol-2-yl)-3-oxo-3-phenylpropanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl benzoylacetate | HCID 7170 | — |
| 반응물 | 2-Amino-6-methoxybenzothiazole | HCID 15630 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | N-(6-methoxybenzothiazol-2-yl)-3-oxo-3-phenylpropanamide | HCID 19975336 | — |
반응 단계
Ethyl benzoyl acetate (9.5 ml) and 2-amino-6-methoxy benzothiazole (9.01 g) are heated to 140° under house vacuum for 2 hours. After cooling, the residue is taken up in acetone and filtered. The precipitate is dissolved in hot DMF to give an amide, N-(6-methoxybenzothiazol -2-yl)-3-oxo-3-phenylpropanamide (II).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05412141 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-05a90fbe55264688b82f73bcc6384ff0 |
| 출처 메모 | uspto-grants-1995_05 |