Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl piperazin-1-ylacetate → N-4-cyanobenzoyl-beta-phenyl-alpha,alpha-dimethyl-beta-alanyl-4-piperazineacetic acid benzyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl piperazin-1-ylacetate | HCID 18423308 | — |
| 반응물 | N-4-cyanobenzoyl-beta-phenyl-alpha,alpha-dimethyl-beta-alanine | HCID 70199446 | — |
| 생성물 | N-4-cyanobenzoyl-beta-phenyl-alpha,alpha-dimethyl-beta-alanyl-4-piperazineacetic acid benzyl ester | HCID 86753675 | 71.9% |
반응 단계
The same procedure as in Example 2-(6-2) was performed with N-4-cyanobenzoyl-β-phenyl-α,α-dimethyl-β-alanine (0.4 g, 1.24 mmol) and piperazineacetic acid benzyl ester (0.87 g, 3.72 mmol) to yield an oil of N-4-cyanobenzoyl-β-phenyl-α,α-dimethyl-β-alanyl-4-piperazineacetic acid benzyl ester (0.48 g, 70.0%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05866592 |
| 출처 데이터셋 | uspto-grants-1999_02 |
| ORD ID | ord-9cc90c3a9f09425c8baf43a68fd29469 |
| 출처 메모 | uspto-grants-1999_02 |