Isobutyraldehyde → isobutyraldehyde AEEA

반응식

[CH:1](=[O:5])[CH:2]([CH3:4])[CH3:3].[NH2:6][CH2:7][CH2:8][CH:9]([CH2:11][NH2:12])[OH:10]>>[CH:1](=[O:5])[CH:2]([CH3:4])[CH3:3].[NH2:6][CH2:7][CH2:8][CH:9]([CH2:11][NH2:12])[OH:10]

참가 물질

반응물 2

HCID 6561Isobutyraldehyde2회

HCID 1646562-Hydroxyputrescine2회

생성물 1

HCID 131718993isobutyraldehyde AEEA

실험 절차

In a typical experiment, isobutyraldehyde and aminoethylethanolamine (AEEA) were pumped separately from weighed feed tanks using adjustable metering pumps. Isobutyraldehyde was pumped at a rate of 0.29 lb/hr and AEEA at a rate of 0.37 lb/hr, giving an isobutyraldehyde/AEEA feed mole ratio of approximately 1.10/1 and a liquid hourly space velocity of 0.5 g total liquid feed/hr/ml catalyst. The two liquid feeds were brought together and allowed to react in a 6-foot coil of 1/4-inch tubing before entering the main reactor. Maximum temperature in this coil of tubing was 64° C.

출처 및 근거

ORD 기록: ord-7272e15fad8f4ddf9923bfd3f29c70c0
출처 데이터셋: uspto-grants-1995_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05414087

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