Azobisisobutyronitrile → Allyl methacrylate

HRID 364158

반응식

HRID 364158 반응식
C(N1C[CH2:6][CH2:5][C:4]1=[O:8])=C.[C:9](OC(C)(C)C)(=[O:13])[C:10]([CH3:12])=[CH2:11].N(C(C)(C)C#N)=NC(C)(C)C#N>O>[C:9]([O:6][CH2:5][CH:4]=[CH2:8])(=[O:13])[C:10]([CH3:12])=[CH2:11]

참가 물질

6

반응물 4

HCID 6547AzobisisobutyronitrileHCID 6917N-vinyl-2-pyrrolidoneHCID 11448tert-Butyl methacrylateHCID 178435178HCID 178435178, 화합물

생성물 1

HCID 7274Allyl methacrylate

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

The dimer of allyl methacrylate, which was prepared according to Example 1, was added to the mixture containing 97 wt.-% N-vinylpyrrolidone and 3 wt.-% tert-butyl methacrylate in the amount of 1 wt. % on the whole mixture. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 90 wt.-% water at G=0.038 MPa.

후처리

  1. additionwas added to the mixture

출처 및 근거

ORD 기록
ord-fa4cadfbf86f465b86bc3bbc95423f31
출처 데이터셋
uspto-grants-1986_08
특허 번호
US04604440

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