Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloro-N,N-diethylbenzamide → n,n-Diethyl-2-chloro-6-[tris(1-methylethyl)silyl]benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 반응물 | Triisopropylsilyl chloride | HCID 139400 | — |
| 생성물 | n,n-Diethyl-2-chloro-6-[tris(1-methylethyl)silyl]benzamide | HCID 18630226 | — |
반응 단계
The title compound was prepared according to General Method A from the compound of Example e and 1.1 eq triisopropylsilyl chloride. Purification by HPLC using 1:19 ethyl acetate/hexanes gave 5.5 g of the desired product as of a clear oil, a 75% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06133252 |
| 출처 데이터셋 | uspto-grants-2000_10 |
| ORD ID | ord-f98a978f36cf430589d464139686e700 |
| 출처 메모 | uspto-grants-2000_10 |