Phosphoric Acid → HCID 131722131, 화합물

HRID 369518노트

반응식

HRID 369518 반응식
[Cl:1][C:2]1[C:3]([CH3:7])=[N:4][NH:5][CH:6]=1.[P:8](=[O:12])([OH:11])([OH:10])[OH:9]>O>[P:8]([O-:12])([OH:11])([OH:10])=[O:9].[Cl:1][C:2]1[CH:6]=[NH+:5][NH:4][C:3]=1[CH3:7]

참가 물질

4

반응물 2

HCID 1004Phosphoric Acid2회HCID 178434543HCID 178434543, 화합물

생성물 1

HCID 131722131HCID 131722131, 화합물수율 98%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

116 g (1.0 mol) of 4-chloro-3-methylpyrazole were dissolved in 115 g (1.0 mol) of phosphoric acid (85%) at room temperature. The water contained in the phosphoric acid was evaporated. After a few hours, the title compound crystallized out of the oil initially present (yield 98%).

후처리

  1. customwas evaporated
  2. waitAfter a few hours
  3. customthe title compound crystallized out of the oil initially present (yield 98%)

출처 및 근거

ORD 기록
ord-faf5b0c53dfd4f30b4bd25cd27ea91c4
출처 데이터셋
uspto-grants-2000_10
특허 번호
US06139596

반응 노트

불러오는 중…