p-n-Octadecyloxybenzoic acid → HCID 18521013, 화합물

HRID 369537

반응식

HRID 369537 반응식
O.[OH-].[Li+].[CH2:4]([O:22][C:23]1[CH:31]=[CH:30][C:26]([C:27]([OH:29])=[O:28])=[CH:25][CH:24]=1)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13]CCCCCCCC>CO>[CH2:4]([O:22][C:23]1[CH:24]=[CH:25][C:26]([C:27]([OH:29])=[O:28])=[CH:30][CH:31]=1)/[CH:5]=[CH:6]/[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

참가 물질

4

반응물 2

HCID 139993p-n-Octadecyloxybenzoic acidHCID 168937Lithium hydroxide, monohydrate

생성물 1

HCID 18521013HCID 18521013, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The ester 35 g 565 mg, 1.95 mmol), and lithium hydroxide monohydrate (817 mg, 19.5 mmol) in 20 ml methanol were reacted according to the procedure for compound 36a. The yield was 482 mg (89% of a white powder.

출처 및 근거

ORD 기록
ord-4f99fb4124484d709c27fecd5c085d15
출처 데이터셋
uspto-grants-2000_10
특허 번호
US06139771

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