Phosphorus tribromide → 3-Cyclopentylbenzyl bromide

HRID 369791노트

반응식

HRID 369791 반응식
[CH:1]1([C:6]2[CH:7]=[C:8]([CH:11]=[CH:12][CH:13]=2)[CH2:9]O)[CH2:5][CH2:4][CH2:3][CH2:2]1.P(Br)(Br)[Br:15]>C(Cl)Cl>[CH:1]1([C:6]2[CH:7]=[C:8]([CH:11]=[CH:12][CH:13]=2)[CH2:9][Br:15])[CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

4

반응물 2

HCID 24614Phosphorus tribromideHCID 537885933-Cyclopentylbenzyl alcohol

생성물 1

HCID 183524773-Cyclopentylbenzyl bromide수율 100%

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

According to example 17, 5.77 g of 3-cyclopentylbenzyl alcohol was treated with 1.09 mL of PBr3 in 25 mL of anhydrous CH2Cl2 to afford 7.85 g (100%) of 3-cyclopentylbenzyl bromide as a light yellow liquid.

출처 및 근거

ORD 기록
ord-ef58c595a3c144afa4f084fa3c0a633c
출처 데이터셋
uspto-grants-2000_10
특허 번호
US06140100

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