Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
7-Methylisatin → HCID 13519800, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 7-Methylisatin | HCID 14313 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 용매 | 1,1-Dichloroethane | HCID 6365 | — |
| 생성물 | HCID 13519800 | HCID 13519800 | — |
반응 단계
The 7-methylisatin (16.1 g, 0.1 mole) is suspended in dichloroethane (2000 ml) and the suspension is heated and irradiated with a high intensity light source to the reflux point. Bromine (24.3 g, 0.15 mole) is added dropwise over a one hour period.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04530929 |
| 출처 데이터셋 | uspto-grants-1985_07 |
| ORD ID | ord-ff59d6552f17494db82c24337df43ee5 |
| 출처 메모 | uspto-grants-1985_07 |