Benzene → Glycine, N-acetyl-N-phenyl-

반응식

[C:1]([OH:5])(=[O:4])[CH:2]=O.[C:6](#[N:8])[CH3:7].[CH:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.S(=O)(=O)(O)[OH:16]>>[C:6]([N:8]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:2][C:1]([OH:5])=[O:4])(=[O:16])[CH3:7]

참가 물질

반응물 4

HCID 241Benzene

HCID 760Glyoxylic Acid

HCID 1118Sulfuric Acid

HCID 6342Acetonitrile

생성물 1

HCID 68483Glycine, N-acetyl-N-phenyl-

실험 절차

Procedure is as in Example 1, but with 195 g (2 moles) of 76% glyoxylic acid, 560 ml of concentrated sulfuric acid, 82 g (2 moles) of acetonitrile and 760 g (10 moles) of benzene and a duration of only 6 hr. 15 min.

후처리

customa duration of only 6 hr
custom15 min.

출처 및 근거

ORD 기록: ord-496708adcc764f3ea4963559af29512c
출처 데이터셋: uspto-grants-1978_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04088657

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