Hydrochloric Acid → HCID 19812359, 화합물

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[C:1]([C:3]1[C:4]([N:16]2[CH2:21][CH2:20][O:19][CH2:18][CH2:17]2)=[N:5][CH:6]=[C:7]([C:9]2[CH:14]=[CH:13][N+:12]([O-:15])=[CH:11][CH:10]=2)[CH:8]=1)#[N:2].C(O)(C)C.CCOCC.[ClH:31]>>[ClH:31].[C:1]([C:3]1[C:4]([N:16]2[CH2:21][CH2:20][O:19][CH2:18][CH2:17]2)=[N:5][CH:6]=[C:7]([C:9]2[CH:10]=[CH:11][N+:12]([O-:15])=[CH:13][CH:14]=2)[CH:8]=1)#[N:2]

참가 물질

반응물 4

HCID 313Hydrochloric Acid

HCID 3283Diethyl Ether

HCID 3776Isopropanol

HCID 10401503HCID 10401503, 화합물

생성물 1

HCID 19812359HCID 19812359, 화합물

실험 절차

1 g 3-Cyano-2-morpholino-5,4'-bipyridine-1'-oxide is dissolved in 5 ml 2N HCl and mixed under cooling with isopropanol and ether, filtered off with suction and dried at 100° C. Yield: 0.9 g (79.8% of the theoretical yield), with a melting point of 222° C.-223° C.

후처리

additionmixed
filtrationfiltered off with suction
customdried at 100° C
customYield: 0.9 g (79.8% of the theoretical yield), with a melting point of 222° C.-223° C.

출처 및 근거

ORD 기록: ord-cf9c751a9c25442c8f844523fd4d709b
출처 데이터셋: uspto-grants-1992_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05162533

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