1-Phenylpiperazine → HCID 19433570, 화합물

HRID 37368

반응식

HRID 37368 반응식
[C:1]1([N:7]2[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:13]([OH:23])(=[O:22])[C:14]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)=[CH2:15]>C(O)C>[C:1]1([N:7]2[CH2:12][CH2:11][N:10]([CH2:15][CH:14]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[C:13]([OH:23])=[O:22])[CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

4

반응물 2

HCID 70961-PhenylpiperazineHCID 68114Atropic acid

생성물 1

HCID 19433570HCID 19433570, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

1-Phenylpiperazine and atropic acid in ethanol is heated under reflux for 18 h, cooled to room temperature, and evaporated in vacuo. The solid is triturated with acetone to give the title product.

후처리

  1. temperatureunder reflux for 18 h
  2. customevaporated in vacuo
  3. customThe solid is triturated with acetone

출처 및 근거

ORD 기록
ord-ddfe5d50e0a74f92b0510bc2dfbdf66c
출처 데이터셋
uspto-grants-1995_05
특허 번호
US05420278

연결된 노트

불러오는 중…