Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 3,4-Dimethylanisole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 3,4-Dimethylphenol | HCID 7249 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 3,4-Dimethylanisole | HCID 78411 | 81% |
반응 단계
To 3,4-dimethylphenol(19.3 g, 0.16 mol), methanol(150 ml) and KOH(9.65 g, 0.25 mol) were added and then refluxed for 2 hrs. Methyl iodide(36.5 g, 0.25 mol) was added thereto, refluxed for 3 hours and then followed by addition of water(150 ml). The resulting mixture was extracted with ethylacetate and purified by column chromatography to obtain the titled compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06028195 |
| 출처 데이터셋 | uspto-grants-2000_02 |
| ORD ID | ord-ec61f0ce6933474899cf676405e5abcb |
| 출처 메모 | uspto-grants-2000_02 |