Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
[3,4-Bis(methoxymethoxy)]phenacyl chloride → HCID 18367762, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | [3,4-Bis(methoxymethoxy)]phenacyl chloride | HCID 18367805 | — |
| 반응물 | 4-Chloro-2-[(ethoxycarbonyl)amino]benzonitrile | HCID 18367888 | — |
| 생성물 | HCID 18367762 | HCID 18367762 | — |
반응 단계
The title compound was prepared according to the procedure described in step 2 of Example 1 from 4-chloro-2-(ethoxycarbonylamino)benzonitrile (Example 1, step 1) and [3,4-bis(methoxymethyloxy)]phenacyl chloride (step 1). 1H-NMR (CDCl3) δ: 8.25 (1H, d, J=1.8 Hz), 7.61 (1H, d, J=2.2 Hz), 7.52 (1H, d, J=8.0 Hz), 7.39 (1H, dd, J=8.4, 1.8 Hz), 7.29 (1H, dd, J=8.4, 1.8 Hz), 7.18 (1H, d, J=8.4 Hz), 5.72 (2H, br s), 5.29 (2H, s), 5.25 (2H, s), 3.86 (2H, q, J=7.3 Hz), 3.52 (6H, s), 0.91 (3H, t, J=7.3 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06300363B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-dbbfe8ad8a194b5182654b6774b19ae1 |
| 출처 메모 | uspto-grants-2001_10 |