Chlorotrimethylsilane → 4-Benzyloxybenzyl chloride

HRID 382391

반응식

HRID 382391 반응식
[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13]O)=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Cl:17][Si](C)(C)C>CS(C)=O>[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][Cl:17])=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 6397ChlorotrimethylsilaneHCID 70043(4-(Benzyloxy)phenyl)methanol

생성물 1

HCID 700424-Benzyloxybenzyl chloride

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

실험 절차

A reaction and post-treatment were carried out following the conditions of Example 71 using 3 g (14 mmol) of 4-benzyloxybenzyl alcohol, 80 ml of chlorotrimethylsilane, 1.09 ml of dimethylsulfoxide, to obtain 4-benzyloxybenzyl chloride.

후처리

  1. customA reaction

출처 및 근거

ORD 기록
ord-5c62664dda0a49dfaeedfe28984ce662
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06310070B1

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