Styrene → GDMA Styrene

HRID 382655

반응식

HRID 382655 반응식
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH2:9]([O:16][C:17]([CH2:19][SH:20])=[O:18])[CH2:10][O:11][C:12]([CH2:14][SH:15])=[O:13]>>[CH2:10]([O:11][C:12]([CH2:14][SH:15])=[O:13])[CH2:9][O:16][C:17]([CH2:19][SH:20])=[O:18].[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 7501Styrene2회HCID 61059Ethylene di(S-thioacetate)

생성물 1

HCID 131721770GDMA Styrene

실험 절차

Styrene (481.4 g, 4.62 eq.) was weighed into a 2000 ml, three neck, round bottom flask along with TPO (1.52 g). The flask was sealed with rubber stoppers and placed in a 60° C. oven for approximately 20 minutes. The contents were swirled occasionally until the TPO dissolved into the styrene. The flask was removed from the oven and allowed to cool to less than 40° C. at which point GDMA (518.6 g, 4.467 eq.) was weighed into the flask.

후처리

  1. customThe flask was sealed with rubber stoppers
  2. customplaced in a 60° C.
  3. customfor approximately 20 minutes
  4. customThe flask was removed from the oven

출처 및 근거

ORD 기록
ord-518ed148ec3b4428a40b53509f42f34c
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06310161B1

연결된 노트

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