Hydrochloric Acid → HCID 67166308, 화합물

HRID 385989

반응식

HRID 385989 반응식
[NH2:1][C:2]([CH:4]1[CH2:9][O:8][CH2:7][CH2:6][N:5]1C(OC(C)(C)C)=O)=[O:3].O1CCOCC1.[ClH:23]>>[ClH:23].[NH:5]1[CH2:6][CH2:7][O:8][CH2:9][CH:4]1[C:2]([NH2:1])=[O:3]

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 312751,4-DioxaneHCID 21098189tert-Butyl 3-carbamoylmorpholine-4-carboxylate

생성물 1

HCID 67166308HCID 67166308, 화합물

실험 절차

1,1-Dimethylethyl 3-(aminocarbonyl)morpholine-4-carboxylate (0.48 g, 2.085 mmol) was taken up in 4 M HCl in dioxane (5 mL, 10.00 mmol) and maintained at room temperature overnight. The solvent was removed in vacuo to afford the title compound as a pale yellow solid.

후처리

  1. customThe solvent was removed in vacuo

출처 및 근거

ORD 기록
ord-11ae47b014e3454b84fe5e46e12c8be8
출처 데이터셋
uspto-grants-2013_02
특허 번호
US08367706B2

연결된 노트

불러오는 중…