Sodium Iodide → HCID 66732740, 화합물

HRID 389002

반응식

HRID 389002 반응식
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[I-].[Na+].[OH-].[Na+].Cl[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][OH:27]>O>[C:3]1([C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=1[O:1][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][OH:27]

참가 물질

6

반응물 4

HCID 5238Sodium IodideHCID 7017(1,1'-Biphenyl)-2-olHCID 14798Sodium HydroxideHCID 900121-Octanol, 8-chloro-

생성물 1

HCID 66732740HCID 66732740, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

The compound was prepared using essentially the procedure of Preparatory Example 1 with 2-hydroxy biphenyl (40 g.), water (250 g.), sodium iodide (3.5 g.) and sodium hydroxide (37.6 g. of 50% in water). This mixture was heated to 100° C. with agitation and 8-chloro-1-octanol (77.4 g.) was added. The product was recovered essentially as in Preparatory Example 1.

후처리

  1. customThe compound was prepared
  2. additionwas added
  3. customThe product was recovered essentially as in Preparatory Example 1

출처 및 근거

ORD 기록
ord-05054416c02248f89e5b132dca5599b6
출처 데이터셋
uspto-grants-2013_02
특허 번호
US08378046B2

연결된 노트

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