Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl mercaptan → 1-Benzylsulfanyl-3-bromo-2-trifluoromethyl-benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl mercaptan | HCID 7509 | — |
| 반응물 | 2-Bromo-6-fluorobenzotrifluoride | HCID 2773345 | — |
| 생성물 | 1-Benzylsulfanyl-3-bromo-2-trifluoromethyl-benzene | HCID 67155259 | — |
반응 단계
Phenyl-methanethiol (4.g g, 37.0 mmol) was treated with commercially available 1-bromo-3-fluoro-2-trifluoromethyl-benzene (10.0 g, 41.1 mmol) in close analogy to the procedure described in step 5.3). The crude product (10.5 g) after workup was used as such in the next reaction step without purification by chromatography.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08378092B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-e82cb9c16d524ad382d59b2d011bdb18 |
| 출처 메모 | uspto-grants-2013_02 |