Methyl iodide → Quinolinium, 1-methyl-, iodide (1:1)
반응식
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[CH3:11][I:12]>O1CCOCC1>[I-:12].[CH3:11][N+:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1참가 물질
4
반응 조건
- 온도
- 150 °C
실험 절차
N-methylquinolinium iodide (Compound III) was synthesized according to the description in the aforementioned reference. Specifically, 2.4 mL of quinoline and 4 mL of methyl iodide were added to 42 mL of anhydrous dioxane, which was stirred at 150° C. for one hour. Thereafter, it was filtered and thereby a precipitate was collected and then washed with ether and petroleum ether. This was dried and thus N-methylquinolinium iodide (Compound III) was obtained.
후처리
- customN-methylquinolinium iodide (Compound III) was synthesized
- filtrationThereafter, it was filtered
- customa precipitate was collected
- washwashed with ether and petroleum ether
- customThis was dried
출처 및 근거
- ORD 기록
- ord-6af5ef6efe2a4092938a0c01e49a2c54
- 출처 데이터셋
- uspto-grants-2013_02
- 특허 번호
- US08383792B2
반응 노트
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