Octyltrichlorosilane → HCID 13977504, 화합물

HRID 395241

반응식

HRID 395241 반응식
[C:1]([O-:4])(=[O:3])[CH3:2].[Na+].[CH2:6]([Si:14](Cl)(Cl)Cl)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]>CCCCCCC>[CH2:6]([Si:14]([O:4][C:1](=[O:3])[CH3:2])([O:3][C:1](=[O:4])[CH3:2])[O:3][C:1](=[O:4])[CH3:2])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

참가 물질

4

반응물 2

HCID 21354OctyltrichlorosilaneHCID 517045Sodium Acetate

생성물 1

HCID 13977504HCID 13977504, 화합물수율 88%

시약·촉매·용매 1

HCID 8900Heptane용매

실험 절차

In a 1-1 round-bottomed flask were placed first 55 g of anhydrous sodium acetate, and then 500 ml of anhydrous heptane. To the white suspension formed was added 50 g of octyltrichlorosilane. The reaction medium was left under stirring at ambient temperature for 2 h, and then filtered under argon to remove the precipitate. The filtrate was concentrated to eliminate the heptane, giving 54 g (88% yield) of octyltriacetoxysilane as a colorless oil.

후처리

  1. customTo the white suspension formed
  2. waitThe reaction medium was left
  3. filtrationfiltered under argon
  4. customto remove the precipitate
  5. concentrationThe filtrate was concentrated

출처 및 근거

ORD 기록
ord-4ac068724ab44b20bce208aa01a6c954
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605423B2

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