Benzoyl chloride → N1-Benzoyl-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine

HRID 395768노트

반응식

HRID 395768 반응식
[C:1](Cl)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:10]([C:14]1[CH:29]=[CH:28][C:17]([C:18]([NH:20][C:21]2[C:22]([NH2:27])=[CH:23][CH:24]=[CH:25][CH:26]=2)=[O:19])=[CH:16][CH:15]=1)([CH3:13])([CH3:12])[CH3:11]>>[C:1]([NH:27][C:22]1[C:21]([NH:20][C:18](=[O:19])[C:17]2[CH:28]=[CH:29][C:14]([C:10]([CH3:12])([CH3:11])[CH3:13])=[CH:15][CH:16]=2)=[CH:26][CH:25]=[CH:24][CH:23]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 7412Benzoyl chlorideHCID 1133079N-(2-aminophenyl)-4-tert-butylbenzamide

생성물 1

HCID 10833099N1-Benzoyl-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine수율 54%

실험 절차

Using the procedure described in Example 93, Part A, benzoyl chloride (0.80 mmol) and N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (0.75 mmol) yielded 150 mg (54%) of the title compound.

출처 및 근거

ORD 기록
ord-675a6bbec5674f09bd5f565ee36bfccb
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605626B2

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