p-Anisoyl chloride → N1-(4-Methoxybenzoyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine

HRID 395769노트

반응식

HRID 395769 반응식
[C:1](Cl)(=[O:10])[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=1.[C:12]([C:16]1[CH:31]=[CH:30][C:19]([C:20]([NH:22][C:23]2[C:24]([NH2:29])=[CH:25][CH:26]=[CH:27][CH:28]=2)=[O:21])=[CH:18][CH:17]=1)([CH3:15])([CH3:14])[CH3:13]>>[CH3:9][O:8][C:5]1[CH:6]=[CH:7][C:2]([C:1]([NH:29][C:24]2[C:23]([NH:22][C:20](=[O:21])[C:19]3[CH:30]=[CH:31][C:16]([C:12]([CH3:14])([CH3:13])[CH3:15])=[CH:17][CH:18]=3)=[CH:28][CH:27]=[CH:26][CH:25]=2)=[O:10])=[CH:3][CH:4]=1

참가 물질

3

반응물 2

HCID 7477p-Anisoyl chlorideHCID 1133079N-(2-aminophenyl)-4-tert-butylbenzamide

생성물 1

HCID 10597246N1-(4-Methoxybenzoyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine수율 61%

실험 절차

Using the procedure described in Example 93, Part A, 4-anisoyl chloride (2.2 mmol) and N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (1.8 mmol) yielded 441 mg (61%) of the title compound.

출처 및 근거

ORD 기록
ord-66dc74ce96ac40648f8c346fa8bab8dc
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605626B2

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