Carbon tetrabromide → (Bromomethyl)cycloheptane

HRID 397683노트

반응식

HRID 397683 반응식
[CH:1]1([CH2:8]O)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(Br)(Br)(Br)[Br:11]>>[Br:11][CH2:8][CH:1]1[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

3

반응물 2

HCID 11205Carbon tetrabromideHCID 78193Cycloheptanemethanol

생성물 1

HCID 23000753(Bromomethyl)cycloheptane

실험 절차

The subtitle compound was prepared by the method of Preparation 9 from cycloheptylmethanol and carbon tetrabromide. The crude product was purified by fractional distillation, b.pt. 115° C.-120° C. @ 30mmHg to afford 1-(bromomethyl)cycloheptane as an oil.

후처리

  1. distillationThe crude product was purified by fractional distillation, b.pt. 115° C.-120° C.

출처 및 근거

ORD 기록
ord-082a997b385e4a4ea28cd2683bd2593d
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06610707B1

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